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SODIUM METHOXIDE 30% SOLUTION

SODIUM METHOXIDE 30% SOLUTION product is 30wt.% solution of sodium methoxide in methanol.

Remarks

Sodium Methoxide,  30% w/w in Methanol

Chemical Properties

Formula                              CH3ONa
Melting point <6°
Formula Weight 54.02
Boiling Point 93°C
Density 0.969
Solubility Miscible with ethanol, fats and esters. Immiscible with hydrocarbons and organic solvents.
Storage & Sensitivity Moisture Sensitive. Air Sensitive. Store under Nitrogen. Ambient temperatures.
SODIUM METHOXIDE SOLUTION
Test Results

Description

Clear colourless liquid
Miscibility
Miscible with Methanol
Assy % (w/w)
29.00 - 31.00
NAOH & NA2CO3AS H2O (Free Alkali)*
0.20% Max.
NAOH & NA2CO3AS NAOH (Free Alkali)
0.44% Max.
* Free water below 1000 PPM.
Note

Air, moisture and heat sensitive. Incompatible with acids, acid chlorides, acid anhydrides, oxidizing agents, alkali metals, chlorinated solvents, water and reducing agents.

GHS Hazard and Precautionary Statements

Hazard Statements:

H226-H290-H301+H311+H331-H314-H370

Flammable liquid and vapour. May be corrosive to metals. Toxic if swallowed. Toxic in contact with skin. Toxic if inhaled. Causes severe skin burns and eye damage. Causes damage to organs.

Precautionary Statements:

P241-P242-P264b-P270-P271-P280-P304+P340-P305+P351+P338-P310-P330-P331-P363-P370+P378r-P390-P402-P403+P233-P405-P406b-P501c

Use explosion-proof electrical/ventilating/lighting/ equipment. Use only non-sparking tools. Wash face, hands and any exposed skin thoroughly after handling Do not eat, drink or smoke when using this product. Use only outdoors or in a well-ventilated area. Wear protective gloves/protective clothing/eye protection/face protection. IF INHALED: Remove to fresh air and keep at rest in a position comfortable for breathing. IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. Immediately call a POISON CENTER or doctor/physician. Rinse mouth. Do NOT induce vomiting. Wash contaminated clothing before reuse. In case of fire: Absorb spillage to prevent material damage. Store in a dry place. Store in a well-ventilated place. Keep container tightly closed. Store locked up. Store in corrosive resistant polypropylene container with a resistant inliner Dispose of contents/ container to an approved waste disposal plant

 

1

MARTERIAL

Sodium Methylate solution in Methanol

2

CHEMICAL FORMULA

CH3ONa:2.333CH3OH

3

STATE

Liquid

4

COLOUR

Colourless to water white

5

ODOUR

Peculiar Sweet smell having some sort of Methanolic tint

6

CLARITY

Clear to slightly turbid with slight haziness, which settles on long standing

7

STRENGTH (CONCENTRATION)

Minimum 30% (W/W)

8

BOILING POINT

93°C (Approximately)

9

CH3ONa (100% REAL)

CONTENT/BARREL

54.00 (+ 0.500) kgs / Barrel

(180.000 kgs/Barrel)

10

CH3ONa:2.333CH3OH (30%W/W)

CONTENT/BARREL

180.000 Kgs/Barrel

11

CH3OH (VIRGIN)

CONTENT/BARREL

126.00 Kgs/Barrel

13

PURITY OF CH3ONa

99.00 % W/W (Minimum)

99.50 % W/W (Maximum)

14

CAUSTIC CONTENT (as NaOH)

00.50 % W/W (Maximum)

15

CARBONATE CONTENT (as Na2CO3)

00.10 % W/W (Maximum)

16

MOISTURE CONTENT (as H2O)

(Theoretical value)

00.50 % W/W (Maximum)

17

pH

Highly Alkaline

18

NOTE

Colour shown by the solution except water-white colour is solely due to packaging material.

19

TESTING STANDARDS

We follow the Testing Standards and Methods set out by the reputed Multinational Companies. For synchronization of Testing results we provide our testing methods or we shall welcome YOUR Specifications and Testing Methods.

20

COMPOSITION PER BARREL

  1. CH3ONa (100% REAL)
  2. CH3OH (VIRGIN)
  3. CH3ONa:2.3333CH3OH

 

  54.00 Kgs

126.00 Kgs

180.00 Kgs.

 

SODIUM METHOXIDE 30% SOLUTION reaction with unactivated aryl bromides in the presence of copper catalyst under various reaction conditions has been studied. It reacts with aryl halides in the presence of a palladium catalyst in DMF (Dimethylformamide) to afford arenes.

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